Publications

SAXS and in-situ SAXS to follow the structural evolution in hybrid materials

Author(s)
Silvia Pabisch, Harald Rennhofer, Nicola Hüsing, Herwig Peterlik
Abstract

The paper focuses on the evolution of oriented nanostructures: An orientation in real space leads to scattering intensities with a preferred orientation with respect to the azimuthal angle in reciprocal space. Thus, the macroscopic orientation of nanostructures can be obtained from SAXS patterns. The additional advantage of in-situ SAXS is that one can directly follow the development of orientated nanostructures during thermal treatment, under extreme conditions or during processing. This is shown in the following for an orientational change of pores in two very different systems, the first being the formation of pores within carbon fibers during loading at high temperatures up to 2000 °C and the second is the development of macroscopically aligned pores in mesostructured silica in the sol-gel process during shear.

Organisation(s)
Dynamics of Condensed Systems
External organisation(s)
Paris-Lodron Universität Salzburg, University of Natural Resources and Life Sciences
Volume
1754
Pages
3-12
No. of pages
10
DOI
https://doi.org/10.1557/opl.2015.587
Publication date
2015
Peer reviewed
Yes
Austrian Fields of Science 2012
103015 Condensed matter, 103009 Solid state physics
ASJC Scopus subject areas
Materials Science(all), Condensed Matter Physics, Mechanical Engineering, Mechanics of Materials
Portal url
https://ucrisportal.univie.ac.at/en/publications/saxs-and-insitu-saxs-to-follow-the-structural-evolution-in-hybrid-materials(186bc9ea-7304-4f28-ad2c-b2714da06b87).html